Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Salicylaldehyde → N,N'-Dodecamethylenebis(2-hydroxybenzylamine)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Salicylaldehyde | HCID 6998 | — |
| 반응물 | 1,12-Dodecanediamine | HCID 17727 | — |
| 촉매 | Nickel | HCID 935 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | N,N'-Dodecamethylenebis(2-hydroxybenzylamine) | HCID 4535168 | — |
반응 단계
30.0 g of a bisazomethine prepared from 2 mols of salicylaldehyde and 1 mol of 1,12-diaminododecane and having a melting point of 72°-73° C. are hydrogenated for 2 hours in 300 ml of isopropanol in an autoclave in the presence of 3 g of Raney nickel at 90°-100° C. and under a pressure of 60 atmospheres
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04129556 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-9057bde9aaa04913b95b1cd6bdea6ee3 |
| 출처 메모 | uspto-grants-1978_12 |