Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl bromide → N-[4-(Allylsulfonyl)phenyl]acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | 4-(Acetylamino)benzenesulfinic acid | HCID 412150 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-[4-(Allylsulfonyl)phenyl]acetamide | HCID 20375362 | — |
반응 단계
50 Parts of p-acetylaminophenylsulfinic acid and 25 parts of sodium hydrogen carbonate are suspended in 300 parts of water. While stirring intensely 36 parts of allyl bromide is dripped in within 3 hours at 50° to 60° C. Stirring is continued for another 4 hours at 60° C. 45 parts of p-allylsulfonylacetanilide is obtained with a melting point of 116° to 118° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04129563 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-b7eadcc681184887b4d6356783e873da |
| 출처 메모 | uspto-grants-1978_12 |