Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → 4-(Benzyloxy)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Ethyl 4-(phenylmethoxy)benzoate | HCID 191414 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-(Benzyloxy)benzoic acid | HCID 73880 | — |
반응 단계
To the solution of 0.5 g KOH in 40 ml MeOH, was added 6.5 mmol of ethyl 4-benzyloxybenzoate. After the resulting mixture was refluxed for 4 hrs, the excess methanol was removed. The residue was mixed with 30 ml water and extracted with ether twice. The water solution was acidified with conc. HCl and extracted with ethyl acetate. The ethyl acetate solution was washed with brine and dried. After evaporation of solvent, pure product was obtained in quantitative yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07083832B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-e893d8e4b615491698f2580374c37cef |
| 출처 메모 | uspto-grants-2006_08 |