Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(R)-(+)-1,1,1-trifluoro-2-octyl 4-benzyloxybenzoate → 4-hydroxybenzoic acid (R)-1-trifluoromethyl-heptyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (R)-(+)-1,1,1-trifluoro-2-octyl 4-benzyloxybenzoate | HCID 22850730 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 4-hydroxybenzoic acid (R)-1-trifluoromethyl-heptyl ester | HCID 14549217 | 99% |
반응 단계
2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07083832B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-3687b0a5c976428fb52ff00b4203cdb7 |
| 출처 메모 | uspto-grants-2006_08 |