Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 1-aminocyclopropane-1-carboxylate hydrochloride → Ethyl 1-(3-(tert-butyldimethylsilyloxy)benzylamino)-cyclopropanecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 1-aminocyclopropane-1-carboxylate hydrochloride | HCID 386203 | — |
| 반응물 | 3-(t-Butyldimethylsilyloxy)benzaldehyde | HCID 11207111 | — |
| 생성물 | Ethyl 1-(3-(tert-butyldimethylsilyloxy)benzylamino)-cyclopropanecarboxylate | HCID 59524373 | 87% |
반응 단계
Prepared as in Example 12-1b from 3-(tert-butyldimethylsilyloxy)benzaldehyde (Example 12-1c) and ethyl 1-aminocyclopropanecarboxylate hydrochloride. Yield 87%, colorless liquid. MS 350 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08076491B2 |
| 출처 데이터셋 | uspto-grants-2011_12 |
| ORD ID | ord-13c7b07b03504482a2d5d68005edf232 |
| 출처 메모 | uspto-grants-2011_12 |