Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile → 4-(2-(5-Amino-2-methylphenylamino)-4-chlorooxazol-5-yl)-2,6-dimethylbenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile | HCID 17757346 | — |
| 반응물 | 4-(2-Chlorooxazol-5-yl)benzonitrile | HCID 68443558 | — |
| 반응물 | 4-(2,4-Dichlorooxazol-5-yl)-2,6-dimethylbenzonitrile | HCID 68443575 | — |
| 생성물 | 4-(2-(5-Amino-2-methylphenylamino)-4-chlorooxazol-5-yl)-2,6-dimethylbenzonitrile | HCID 24872115 | 74% |
반응 단계
The same procedure outlined above in the preparation of 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile was used. However 4-(2,4-dichlorooxazol-5-yl)-2,6-dimethylbenzonitrile was used instead 4-(2-Chloro-oxazol-5-yl)-benzonitrile. Yield=74%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08080669B2 |
| 출처 데이터셋 | uspto-grants-2011_12 |
| ORD ID | ord-4ec7fc8e5945464bac93baab64c5e2b7 |
| 출처 메모 | uspto-grants-2011_12 |