3-Phenylpropane-1-thiol → HCID 178420287, 화합물

HRID 660176노트

반응식

HRID 660176 반응식
[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:18][CH2:19][N:14]([CH2:15][CH2:16]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[C:20]1(CCCS)[CH:25]=CC=C[CH:21]=1>>[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:18][CH2:19][N:14]([CH2:15][CH2:16]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH2:2][C:3]1[CH:25]=[CH:20][CH:21]=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 905963-Phenylpropane-1-thiolHCID 178447695HCID 178447695, 화합물

생성물 1

HCID 178420287HCID 178420287, 화합물수율 11%

실험 절차

Compound 49G was prepared following the procedure as described for the synthesis of compound 49B (see Scheme 10) using 3-phenyl-1-propanethiol as reagent. Subsequent purification by flash chromatography (EtOH) afforded compound 49G.

후처리

  1. customSubsequent purification by flash chromatography (EtOH)

출처 및 근거

ORD 기록
ord-87aa1a4fbbde4e599fa645f945ce1bf0
출처 데이터셋
uspto-grants-2011_12
특허 번호
US08084473B2

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