Isoamyl mercaptan → HCID 178447694, 화합물

HRID 660177노트

반응식

[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:18][CH2:19][N:14]([CH2:15][CH2:16]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH2:2][CH2:3][CH2:4]C.[CH3:20]C(C)CCS>>[CH3:20][CH:3]([CH3:4])[CH2:2][CH2:1][S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:16][CH2:15][N:14]([CH2:19][CH2:18]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1

참가 물질

반응물 2

HCID 10925Isoamyl mercaptan

HCID 178447695HCID 178447695, 화합물

생성물 1

HCID 178447694HCID 178447694, 화합물수율 20%

실험 절차

Compound 49H was prepared following the procedure as described for the synthesis of compound 49B (see Scheme 10) using 3-methyl-1-butanethiol as reagent. Subsequent purification by flash chromatography (EtOH) afforded compound 49G.

후처리

customSubsequent purification by flash chromatography (EtOH)

출처 및 근거

ORD 기록: ord-95cf7ed926c34dae8b43c6eb414b5e60
출처 데이터셋: uspto-grants-2011_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08084473B2

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