Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → 7-Chloro-1-methyllepidinium iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 7-Chloro-4-methylquinoline | HCID 170437 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 7-Chloro-1-methyllepidinium iodide | HCID 22016371 | — |
반응 단계
A portion of the 7-chlorolepidine (80 mg) prepared as above was methylated by heating with CH3I (0.5 ml) in CH3CN (1 ml) at reflux for two hours. The mixture was treated with diethyl ether, followed by centrifugation, to give a yellow powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07083982B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-6a873647e2b44ce99055068705e47796 |
| 출처 메모 | uspto-grants-2006_08 |