Thenyl mercaptan → Ethyl-thenyl-disulphide

HRID 66060

반응식

HRID 66060 반응식
[C:1]1([CH2:6][SH:7])[S:5][CH:4]=[CH:3][CH:2]=1.C(N1C(=O)C2=CC=CC=[C:12]2[C:11]1=[S:20])C>>[CH2:11]([S:20][S:7][CH2:6][C:1]1[S:5][CH:4]=[CH:3][CH:2]=1)[CH3:12]

참가 물질

3

반응물 2

HCID 80408Thenyl mercaptanHCID 57251189N-ethylthiophthalimide

생성물 1

HCID 20306424Ethyl-thenyl-disulphide

실험 절차

Starting from thenylmercaptan and N-ethylthiophthalimide there is obtained ethyl-thenyl-disulphide. nD20 = 1.6044. IR (liq.): bands inter alia at 3000, 1450, 1250, 1035, 850, 700 cm-1.

출처 및 근거

ORD 기록
ord-f7e43eeb16844ee88a5127f4425f5366
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04130562

연결된 노트

불러오는 중…