Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dabco → [1,1'-Biphenyl]-3-ylmethyl 3-(2,2-dibromoethenyl)-2,2-dimethycyclopropanecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dabco | HCID 9237 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 3-(2,2-Dibromovinyl)-2,2-dimethylcyclopropane-1-carboxylic acid | HCID 181248 | — |
| 반응물 | 3-(Bromomethyl)biphenyl | HCID 3864405 | — |
| 생성물 | [1,1'-Biphenyl]-3-ylmethyl 3-(2,2-dibromoethenyl)-2,2-dimethycyclopropanecarboxylate | HCID 13064776 | — |
반응 단계
[1,1'-Biphenyl]-3-ylmethyl 3-(2,2-dibromoethenyl)-2,2-dimethycyclopropanecarboxylate was prepared by the method described in Example 1B above using potassium hydroxide (0.66 g, 0.12 mole), 3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylic acid (5.3 g, 0.12 mole), which may be prepared according to the method of Elliott, et al., U.S. Pat. No. 4,024,163, 3-bromomethylbiphenyl (2.7 g, 0.12 mole), and 0.1 g of 1,4-diazabicyclo[2.2.2]octane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04130657 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-3416e62f173340af90f85110cb689995 |
| 출처 메모 | uspto-grants-1978_12 |