2,6-Di-tert-butylphenol → Cyclopropyl(3,5-ditert-butyl-4-hydroxyphenyl)methanone

반응식

[CH:1]1([C:4](Cl)=[O:5])[CH2:3][CH2:2]1.[C:7]([C:11]1[CH:16]=[CH:15][CH:14]=[C:13]([C:17]([CH3:20])([CH3:19])[CH3:18])[C:12]=1[OH:21])([CH3:10])([CH3:9])[CH3:8]>>[CH:1]1([C:4]([C:15]2[CH:14]=[C:13]([C:17]([CH3:18])([CH3:19])[CH3:20])[C:12]([OH:21])=[C:11]([C:7]([CH3:10])([CH3:9])[CH3:8])[CH:16]=2)=[O:5])[CH2:3][CH2:2]1

참가 물질

반응물 2

HCID 314052,6-Di-tert-butylphenol

HCID 77637Cyclopropanecarbonyl chloride

생성물 1

HCID 54172676Cyclopropyl(3,5-ditert-butyl-4-hydroxyphenyl)methanone

실험 절차

Reacting cyclopropanecarbonyl chloride with 2,6-di(t-butyl)phenol by the method of Example 1, white, solid 3,5-di(t-butyl)-4-hydroxyphenyl cyclopropyl ketone, m.p. 140.5°-142.5° C. is obtained.

출처 및 근거

ORD 기록: ord-953e72e7c57b470fa8572f6a34cdf5ce
출처 데이터셋: uspto-grants-1978_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04130666

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