Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dichloroaniline → 3-Benzoyl-2',6'-dichloroacrylanilide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dichloroaniline | HCID 11846 | — |
| 반응물 | Pentafluoroaniline | HCID 13040 | — |
| 반응물 | Phosphorus pentachloride | HCID 24819 | — |
| 반응물 | 2-Benzoylprop-2-enoic acid | HCID 15839051 | — |
| 반응물 | 3-(Benzoyl)pentafluoroacrylanilide | HCID 85847495 | — |
| 생성물 | 3-Benzoyl-2',6'-dichloroacrylanilide | HCID 85847494 | — |
반응 단계
The following additional compounds are prepared by employing PCl5 reagent in accordance with the method of the above Example 6. An analogous quantity of the appropriate benzoylacrylic acid or a substituted benzoylacrylic acid is employed in the manner of the benzoylacrylic acid of Example 5. Likewise, an analogous quantity of the appropriately substituted aniline is employed in the manner of the 2,6-dichloroaniline. Thus, to prepare 3-(benzoyl)pentafluoroacrylanilide, an analogous amount of benzoylacrylic acid is employed and there is used an analogous quantity of pentafluoroaniline in place of the 2,6-dichloroaniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04130661 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-3d7c09b7671b429ca9133e350ed4823e |
| 출처 메모 | uspto-grants-1978_12 |