4-Oxobutanoic acid → Isopropylaminium

HRID 66156

반응식

HRID 66156 반응식
[O:1]=[CH:2][CH2:3][CH2:4][C:5]([OH:7])=[O:6].[CH:8]([NH2:11])([CH3:10])[CH3:9]>C1C=CC=CC=1>[CH:8]([NH3+:11])([CH3:10])[CH3:9].[O:1]=[CH:2][CH2:3][CH2:4][C:5]([O-:7])=[O:6]

참가 물질

5

반응물 2

HCID 11124-Oxobutanoic acidHCID 6363Isopropylamine

생성물 2

HCID 3364502IsopropylaminiumHCID 95432384-Oxobutanoate

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

100 Mg. of 4-(6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyric acid in 15 ml. of hot benzene is treated with 60 mg. of isopropyl amine. The solution is allowed to cool to room temperature and the product is filtered off, washed with ether and dried to yield isopropylammonium 4-(6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyrate.

후처리

  1. filtrationthe product is filtered off
  2. washwashed with ether
  3. customdried

출처 및 근거

ORD 기록
ord-9fbbeabf522d4d0bb714410dabecfb77
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04130654

연결된 노트

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