Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Oxobutanoic acid → 1-Piperidinium
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Oxobutanoic acid | HCID 1112 | — |
| 반응물 | Piperidine | HCID 8082 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 1-Piperidinium | HCID 637969 | — |
| 생성물 | 4-Oxobutanoate | HCID 9543238 | — |
반응 단계
100 Mg. of 4-(8-methoxy-6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyric acid in 10 ml. of benzene is treated with 60 mg. of piperidine. The solution obtained is allowed to stand for one hour and the crystalline material which forms is filtered, washed with ether and air dried to yield piperidinium 4-(8-methoxy-6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyrate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04130654 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-95cdf6991778486985518cab3455bb88 |
| 출처 메모 | uspto-grants-1978_12 |