Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 3,4-Dichlorostyrylsulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 3,4-Dichlorostyrylsulfonyl chloride | HCID 53976486 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3,4-Dichlorostyrylsulfonamide | HCID 53794380 | 97% |
반응 단계
Ammonia is bubbled through a solution of 3,4-dichlorostyrylsulfonyl chloride (27.2 g., 0.1 mole) in 250 ml. of ether for a period of 30 min. at about 20° C. The solvent is evaporated and the residue stirred with water, collected and dried at 100° C. under vacuum affords 24.6 g. (97% yield) of 3,4-dichlorostyrylsulfonamide, m.p. 127°-130° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04130663 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-b239bfe86419420bac159339e2131826 |
| 출처 메모 | uspto-grants-1978_12 |