Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide dimethyl acetal → 1,4,8-Triazatricyclo[6.3.1.04,12]dodecane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 반응물 | 1,4,8-Triazacycloundecane | HCID 398742 | — |
| 생성물 | 1,4,8-Triazatricyclo[6.3.1.04,12]dodecane | HCID 12641658 | 81.8% |
반응 단계
In a manner similar to that of Example 1 (C), 5.28 g (33.6 mmol) of 1,4,8-triazacycloundecane and 4.00 g of dimethylformamide dimethyl acetal were reacted to give 4.59 g of 1,4,8-triazatricyclo[6.3.1.04,12 ]dodecane as a clear, colorless liquid, bp 80°-82° (three fractions) (1.2 mm), nD24 = 1.5182. A fraction boiling at 82° was analyzed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04130715 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-141a818fb3f74ff09394c0b370e6a40e |
| 출처 메모 | uspto-grants-1978_12 |