Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide dimethyl acetal → Hexahydro-1H,4H,7H-3a,6a,9a-triazaphenalene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 반응물 | 1,5,9-Triazacyclododecane | HCID 470778 | — |
| 생성물 | Hexahydro-1H,4H,7H-3a,6a,9a-triazaphenalene | HCID 12641659 | 73.1% |
반응 단계
In a manner similar to that of Example 1 (C), 5.00 g (29.2 mmol) of 1,5,9-triazacyclododecane and 3.48 g of dimethylformamide dimethyl acetal were reacted to give 3.87 g of 1,5,9-triazatricyclo[7.3.1.05,13 ]tridecane as a clear, colorless liquid, bp 93° (three fractions) (0.35 mm), which solidified on standing at room temperature. One fraction was analyzed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04130715 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-d742f01c8a9a451f8198c8a3497b4046 |
| 출처 메모 | uspto-grants-1978_12 |