N1-(Phenylmethyl)-N2-(2-((phenylmethyl)amino)ethyl)-1,2-ethanediamine → 1,7-Dimethylhexahydro-1H-imidazo[1,2-a]imidazole

반응식

C(NCCNCCNCC1C=CC=CC=1)C1C=CC=CC=1.CNCCNCCNC.[CH2:31]([N:38]1[CH:45]2[N:41]([CH2:42][CH2:43][N:44]2[CH2:46]C2C=CC=CC=2)[CH2:40][CH2:39]1)C1C=CC=CC=1>>[CH3:46][N:44]1[CH:45]2[N:41]([CH2:40][CH2:39][N:38]2[CH3:31])[CH2:42][CH2:43]1

참가 물질

반응물 3

HCID 28479N1-(Phenylmethyl)-N2-(2-((phenylmethyl)amino)ethyl)-1,2-ethanediamine

HCID 3706439N,N'-(Iminobisethylene)bismethanamine

HCID 227559294,6-Dibenzyl-1,4,6-triazabicyclo[3.3.0]octane

생성물 1

HCID 126479551,7-Dimethylhexahydro-1H-imidazo[1,2-a]imidazole

실험 절차

If 1,7-dibenzyldiethylenetriamine were substituted for 1,7-dimethyldiethylenetriamine in essentially the procedure of part (A) above, the product would be 4,6-dibenzyl-1,4,6-triazabicyclo[3.3.0]octane, ##STR25##

출처 및 근거

ORD 기록: ord-d2becc03803f4c0092534d140e4e046b
출처 데이터셋: uspto-grants-1978_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04130715

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