Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
9,10-Dimethylanthracene → Anthracene, 9,10-dihydro-9,10-dimethyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 9,10-Dimethylanthracene | HCID 13076 | — |
| 촉매 | HCID 178505374 | HCID 178505374 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Anthracene, 9,10-dihydro-9,10-dimethyl- | HCID 606352 | 8% |
반응 단계
9,10-Dihydro-9,10-dimethylanthracene was prepared by hydrogenation of 9,10-dimethylanthracene with Girdler G-22 copper chromite catalyst in toluene at 120° C. and 1500 psi for 1 hour. The mixtures resulting from five such runs were combined and filtered, and the off-white solid product was isolated by evaporating the solvent. It was characterized by nmr spectroscopy.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04131646 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-33838fd7755847479484c70ff8d9c312 |
| 출처 메모 | uspto-grants-1978_12 |