Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → 3-(1-Adamantylcarbonyl)-1-(p-chlorophenyl)-3-azabicyclo[3.1.0]hexane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 1-Adamantanecarbonyl chloride | HCID 98915 | — |
| 반응물 | 1-(4-Chlorophenyl)-3-azabicyclo[3.1.0]hexane | HCID 10130331 | — |
| 생성물 | 3-(1-Adamantylcarbonyl)-1-(p-chlorophenyl)-3-azabicyclo[3.1.0]hexane | HCID 20468354 | — |
반응 단계
A sample of 19.35 g of 1-p-chlorophenyl-3-azabicyclo[3.1.0]hexane, 10.59 g of sodium carbonate and 19.87 g of 1-adamantanecarboxylic acid chloride are reacted in accordance with Example 36, yielding the product 3-(1-adamantylcarbonyl)-1-(p-chlorophenyl)-3-azabicyclo[3.1.0]hexane as a white solid, mp 163°-165° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04131611 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-7dd1cd11db6b43f6852336020da61547 |
| 출처 메모 | uspto-grants-1978_12 |