참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Tetraethylene Glycol | HCID 8200 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | Methanesulfonate | HCID 85257 | — |
| 반응물 | 1-Phenyl-2,5,8,11-tetraoxatridecan-13-ol | HCID 11076957 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-Phenyl-2,5,8,11,14,17,20,23-octaoxapentacosan-25-ol | HCID 57437703 | 34.5% |
반응 단계
To a solution of tetrahydrofuran (140 mL) containing sodium hydride (0.43 g, 18 mmol) was added dropwise a solution of non-polydispersed tetraethylene glycol (3.5 g, 18 mmol) in tetrahydrofuran (10 mL) and the reaction mixture was stirred for 1 h. Then mesylate of non-polydispersed tetraethylene glycol monobenzylether 40 (6.0 g, 16.5 mmol) dissolved in tetrahydrofuran (10 mL) was added dropwise and the reaction mixture was stirred overnight. The crude reaction mixture was filtered through Celite (washed, CH2Cl2, 250 mL) and the filtrate was washed H2O, dried MgSO4, and evaporated to dryness. The resultant oil was chromatographed (silica, ethyl acetate/methanol, 10:1) and chromatographed (silica, chloroform/methanol, 25:1) to afford the non-polydispersed title compound as a clear oil (2.62 g, 34% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07084121B2 |
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| 출처 데이터셋 | uspto-grants-2006_08 |
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| ORD ID | ord-746ede52140b4ff6b3a407b25a39a3df |
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| 출처 메모 | uspto-grants-2006_08 |
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