Ammonia → N-methyldihydrophenethylamine

HRID 66397

반응식

HRID 66397 반응식
[CH3:1][NH:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[Li].N>C(O)C>[CH3:1][NH:2][CH2:3][CH2:4][CH:5]1[CH:6]=[CH:7][CH:8]=[CH:9][CH2:10]1

참가 물질

5

반응물 3

HCID 222AmmoniaHCID 11503N-MethylbenzeneethanamineHCID 3028194Lithium

생성물 1

HCID 21325368N-methyldihydrophenethylamine

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

46 g. (0.34 moles) of N-methylphenethylamine are reduced by treatment with 16 g. of lithium (2.3 g. atom) in 1.5 1. of ammonia and 250 ml. ethanol according to the procedure of Example 1(a) to yield crude N-methyldihydrophenethylamine.

출처 및 근거

ORD 기록
ord-853d697325634bb4aa8492033409c708
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04131744

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