Piperidine, 1-(2-chloroethyl)-, hydrochloride → 1-[2-Chloro-4-(2-piperidinoethoxy)phenyl]-1-butanone

HRID 66611

반응식

HRID 66611 반응식
[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH2:9][CH2:10][N:11]([CH2:14][CH3:15])[CH2:12][CH3:13])[CH:5]=[CH:4][C:3]=1[C:16](=[O:20])[CH2:17][CH2:18][CH3:19].Cl.Cl[CH2:23]CN1CCCCC1>>[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH2:9][CH2:10][N:11]2[CH2:12][CH2:13][CH2:23][CH2:15][CH2:14]2)[CH:5]=[CH:4][C:3]=1[C:16](=[O:20])[CH2:17][CH2:18][CH3:19]

참가 물질

3

반응물 2

HCID 74826Piperidine, 1-(2-chloroethyl)-, hydrochlorideHCID 130523711-[2-Chloro-4-(2-diethylaminoethoxy)phenyl]-1-butanone

생성물 1

HCID 204971741-[2-Chloro-4-(2-piperidinoethoxy)phenyl]-1-butanone

실험 절차

This compound is prepared by essentially the same procedure as described in Example 1 Step A except that the 2-diethylaminoethyl chloride hydrochloride of Example 1 Step A is replaced by an equimolecular quantity of N-(2-chloroethyl)piperidine hydrochloride. The product is obtained as a pale yellow oil upon distillation in vacuo (0.3 mm.).

후처리

  1. customThis compound is prepared by essentially the same procedure
  2. customThe product is obtained as a pale yellow oil upon distillation in vacuo (0.3 mm.)

출처 및 근거

ORD 기록
ord-ad2f2adcef4341c886b4b3a491aeaed7
출처 데이터셋
uspto-grants-1982_08
특허 번호
US04342782

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