Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 2-(beta-Hydroxypropylthio)nitrobenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | o-Nitrobenzenethiol | HCID 21002 | — |
| 반응물 | 1-Chloro-2-propanol | HCID 31370 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-(beta-Hydroxypropylthio)nitrobenzene | HCID 20530674 | 94.8% |
반응 단계
In accordance with Reaction I of Example 1, 15.5 g. (0.1 mole) of 2-nitrothiophenol, 11.34 g. (0.12 mole) of 1-chloro-2-propanol, 4.0 g. (0.1 mole) of sodium hydroxide and 150 ml. of water were used for the reaction and an oily product was extracted with benzene after the reaction and benzene was distilled off after a dehydration to obtain 20.2 g. of blackish brawn liquid 2-(β-hydroxypropylthio)nitrobenzene (yield of 94.8%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04342859 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-86835705cda74f718b42990acbcada29 |
| 출처 메모 | uspto-grants-1982_08 |