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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 66714생성일: 2026년 10월 26일

Methyl acetoacetate → HCID 178429333, 화합물

https://huagongshe.com/reaction/66714

반응식

참여 물질

역할이름HCID투입량
반응물Methyl acetoacetateHCID 7757—
반응물2,2,2-TrichloroethanimidamideHCID 35608—
반응물Carbamic chlorideHCID 68048—
생성물HCID 178429333HCID 178429333—

반응 단계

The pyrimidinyl carbamate compounds of the present invention may be prepared by reacting trichloroacetamidine with the corresponding acetoacetate to form the corresponding 4-hydroxy-2-trichloromethylpyrimidine, which is then reacted with a selected carbamoyl chloride. These general reactions are illustrated below in equations (A) and (B). In equation (A), trichloroacetamidine is reacted with methylacetoacetate to form 4-hydroxy-6-methyl-2-trichloromethylpyrimidine. In equation (B), the 4-hydroxy-6-methyl-2-trichloromethylpyrimidine is reacted with dimethylcarbamoyl chloride to form 6-methyl-2-trichloromethyl-4-pyrimidinyl dimethylcarbamate. ##STR3##

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04343803
출처 데이터셋uspto-grants-1982_08
ORD IDord-1123ac975f29475ca70fb7029fd9b47f
출처 메모uspto-grants-1982_08