Ammonium Hydroxide → 2-Amino-6-methoxypyrazine 4-oxide

HRID 66742노트

반응식

HRID 66742 반응식
Cl[C:2]1[CH:7]=[N+:6]([O-:8])[CH:5]=[C:4]([O:9][CH3:10])[N:3]=1.[OH-].[NH4+:12]>>[NH2:12][C:2]1[CH:7]=[N+:6]([O-:8])[CH:5]=[C:4]([O:9][CH3:10])[N:3]=1

참가 물질

3

반응물 2

HCID 14923Ammonium HydroxideHCID 205289402-Chloro-6-methoxypyrazine 4-oxide

생성물 1

HCID 205289822-Amino-6-methoxypyrazine 4-oxide

실험 절차

2-Chloro-6-methoxypyrazine 4-oxide is treated with an excess of ammonium hydroxide in an autoclave at 150° C. for 14 hours. The reaction mixture is cooled and evaporated to dryness to give the crude product which may be used in the next step as is.

후처리

  1. temperatureThe reaction mixture is cooled
  2. customevaporated to dryness

출처 및 근거

ORD 기록
ord-75ecce3c4fbf44649962e18d43f73347
출처 데이터셋
uspto-grants-1982_08
특허 번호
US04343802

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