참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-Chlorophthalic anhydride | HCID 67014 | — |
| 반응물 | Potassium Fluoride | HCID 522689 | — |
| 생성물 | 3-Fluorophthalic anhydride | HCID 69551 | 69% |
반응 단계
A mixture of 20 parts of 3-chlorophthalic anhydride, and 20 parts of anhydrous potassium fluoride was heated and maintained at about 235° C. for about 9 hours. The reaction mixture was then cooled and the crude product removed by vaccum distillation and recrystallized from chloroform to yield 12.65 parts of purified 3-fluorophthalic anhydride (69% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04343951 |
|---|
| 출처 데이터셋 | uspto-grants-1982_08 |
|---|
| ORD ID | ord-42b2a6f74dd5429695d292be7a7d85bf |
|---|
| 출처 메모 | uspto-grants-1982_08 |
|---|
