2-Nitropropane → HCID 178430959, 화합물

HRID 66957

반응식

HRID 66957 반응식
[N+:1]([CH:4]([CH3:6])[CH3:5])([O-:3])=O.[CH:7]1[CH:15]=[CH:14][C:13]2[C:9](=[N:10][O:11][N+]=2[O-])[CH:8]=1.C(NCC)C>O1CCCC1>[CH3:5][C:4]1([CH3:6])[N+:1]([O-:3])=[C:13]2[CH:14]=[CH:15][CH:7]=[CH:8][C:9]2=[N+:10]1[O-:11]

참가 물질

5

반응물 3

HCID 3982-NitropropaneHCID 8021DiethylamineHCID 68075Benzofuroxan

생성물 1

HCID 178430959HCID 178430959, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

To a mixture containing 2-nitropropane (10.7 g., 0.12 moles), benzofuroxan (13.6 g., 0.10 moles) and tetrahydrofuran (50 ml.) is added dropwise diethylamine (8.7 g., 0.12 mole). The reaction temperature rises during addition. Upon completion of addition, the reaction mixture is allowed to sit overnight at room temperature.

후처리

  1. additionThe reaction temperature rises during addition
  2. additionUpon completion of addition

출처 및 근거

ORD 기록
ord-1c8ab1a20a294172a812417cba9eb226
출처 데이터셋
uspto-grants-1982_08
특허 번호
US04343942

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