2-Nitropropane → HCID 178430959, 화합물
반응식
[N+:1]([CH:4]([CH3:6])[CH3:5])([O-:3])=O.[CH:7]1[CH:15]=[CH:14][C:13]2[C:9](=[N:10][O:11][N+]=2[O-])[CH:8]=1.C(NCC)C>O1CCCC1>[CH3:5][C:4]1([CH3:6])[N+:1]([O-:3])=[C:13]2[CH:14]=[CH:15][CH:7]=[CH:8][C:9]2=[N+:10]1[O-:11]참가 물질
5
실험 절차
To a mixture containing 2-nitropropane (10.7 g., 0.12 moles), benzofuroxan (13.6 g., 0.10 moles) and tetrahydrofuran (50 ml.) is added dropwise diethylamine (8.7 g., 0.12 mole). The reaction temperature rises during addition. Upon completion of addition, the reaction mixture is allowed to sit overnight at room temperature.
후처리
- additionThe reaction temperature rises during addition
- additionUpon completion of addition
출처 및 근거
- ORD 기록
- ord-1c8ab1a20a294172a812417cba9eb226
- 출처 데이터셋
- uspto-grants-1982_08
- 특허 번호
- US04343942
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