Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzeneacetic acid, 4-chloro-alpha-(1-methylethyl)- → 2-(4-Chlorophenyl)-3-methylbutanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzeneacetic acid, 4-chloro-alpha-(1-methylethyl)- | HCID 16197 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 2-(4-Chlorophenyl)-3-methylbutanoyl chloride | HCID 4178001 | — |
반응 단계
10 g of the product of Step D were added to a mixture of 50 ml of petroleum ether (b.p.=35°-70° C.) and 20 ml of thionyl chloride and the mixture was refluxed for 4 hours and was then cooled. The mixture was evaporated to dryness to obtain 10.8 g of D 2-isopropyl-2-p-chlorophenyl acetyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04344895 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-55d226453b9140adbbf9185143dcf950 |
| 출처 메모 | uspto-grants-1982_08 |