Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl formate → N-formyl-4-(3-azidopropyl)-piperidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl formate | HCID 7865 | — |
| 반응물 | 4-(3'-Azidopropyl)-piperidine | HCID 13503220 | — |
| 생성물 | N-formyl-4-(3-azidopropyl)-piperidine | HCID 13503223 | — |
반응 단계
A solution of 4-(3'-azidopropyl)-piperidine (1.5 g) in methyl formate (5 ml) was refluxed for 1 hour. Evaporation to dryness gave the desired compound as an oil. The IR-spectrum (CHCl3) showed strong bands at 2100, 1660, 1440 and 1270 cm-1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04345071 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-78226627656b46d0aa0bbec9bf151a48 |
| 출처 메모 | uspto-grants-1982_08 |