Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Phenyl-but-3-ynyl)-carbamic acid tert-butyl ester → 4-Phenyl-but-3-ynylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Phenyl-but-3-ynyl)-carbamic acid tert-butyl ester | HCID 23544319 | — |
| 용매 | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| 생성물 | 4-Phenyl-but-3-ynylamine | HCID 15642991 | — |
반응 단계
A solution of (4-phenyl-but-3-ynyl)-carbamic acid tert-butyl ester (98 mg) was stirred for 0.5 h in 1:1 trifluoroacetic acid/dichloromethane (10 ml). The volatile materials were evaporated to give the crude 4-phenyl-but-3-ynylamine, which was used in subsequent transformations without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07084154B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-20d2e46c1d1247a2976c93d528f9a3be |
| 출처 메모 | uspto-grants-2006_08 |