Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclopentadeca-2,14-dien-1-one → Cyclopentadecanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclopentadeca-2,14-dien-1-one | HCID 53676690 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Cyclopentadecanone | HCID 10409 | 94% |
반응 단계
A solution of 1.00 g (4.55 mMole) of cyclopentadeca-2,14-dien-1-one in 20 ml of ethanol was hydrogenated in the presence of 50 mg of palladium on charcoal. Hydrogen uptake (230 ml) was complete after 1 h at 20°. The mixture was filtered, evaporated and distilled to give 0.96 g (94%) of EXALTONE® having b.p. 115°/0.1 Torr; m.p. 65°-66°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346023 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-21dadf26d14a4ba4b795642887de36a9 |
| 출처 메모 | uspto-grants-1982_08 |