Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitromethane → Methyl 4-(2-nitroethenyl)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitromethane | HCID 6375 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Methyl 4-Formylbenzoate | HCID 15294 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 4-(2-nitroethenyl)benzoate | HCID 896295 | — |
반응 단계
Sodium hydroxide (1 N, 2.3 mL) was added dropwise to 4-formyl-benzoic acid methyl ester (0.33 g) and nitromethane (0.11 ml) in 5 mL methanol at 0° C. The solution was acidified after 0.5 h and a precipitate was formed. The precipitate was isolated by filtration to give 228 mg of 4-(2-nitro-vinyl)-benzoic acid methyl ester.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07084154B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-bbf5b318502845ec93a68e348bf67846 |
| 출처 메모 | uspto-grants-2006_08 |