Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 4-isostearamidoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Diethylenetriamine | HCID 8111 | — |
| 반응물 | Ethyl Acetoacetate | HCID 8868 | — |
| 반응물 | 16-Methylheptadecanoic Acid | HCID 21859 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-isostearamidoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one | HCID 131712802 | — |
반응 단계
Into an apparatus similar to that in Example 1, were charged 103.1 g (1 mole) of diethylenetriamine and 284.5 g (1 mole) of isostearic acid. At 200° to 210° C., 18 g of water was distilled off to effect the monoamide formation. Then, after the addition of 130.1 g (1 mole) of ethyl acetoacetate, 18 g of water and 46 g of ethanol were distilled off at 150° to 160° C. to obtain 4-isostearamidoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346087 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-53068da6218c4df7a8839381c2a1f811 |
| 출처 메모 | uspto-grants-1982_08 |