Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(2-Hydroxyethyl)ethylenediamine → HCID 70548023, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(2-Hydroxyethyl)ethylenediamine | HCID 8112 | — |
| 반응물 | Ethyl Acetoacetate | HCID 8868 | — |
| 반응물 | Oleic Acid | HCID 445639 | — |
| 생성물 | HCID 70548023 | HCID 70548023 | — |
반응 단계
Into an apparatus similar to that in Example 1, were charged 104.2 g (1 mole) of N-hydroxyethylethylenediamine and 130.1 g (1 mole) of ethylacetoacetate. At 150° to 160° C., 18 g of water and 46 g of ethanol were distilled off. Then, after addition of 282.5 g (1 mole) of oleic acid, the esterification was effected at 210° to 215° C. to distil off 18 g of water and to obtain 4-oleoyloxyethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346087 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-8269985706b54541bda8fb7aa7663629 |
| 출처 메모 | uspto-grants-1982_08 |