Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(2-Hydroxyethyl)ethylenediamine → 4-Behenoyloxyethyl-2,3,6,7-tetrahydro-1,4-diazocin-5-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(2-Hydroxyethyl)ethylenediamine | HCID 8112 | — |
| 반응물 | Docosanoic Acid | HCID 8215 | — |
| 반응물 | Methyl 4-oxobutyrate | HCID 83779 | — |
| 생성물 | 4-Behenoyloxyethyl-2,3,6,7-tetrahydro-1,4-diazocin-5-one | HCID 54163854 | — |
반응 단계
Into an apparatus similar to that in Example 1, were charged 104.2 g (1 mole) of N-hydroxyethylethylenediamine and 116.1 g (1 mole) of methyl 3-formylpropionate. At 130° C., 18 g of water and 32 g of methanol were distilled off. After adding 340.5 g (1 mole) of behenic acid, esterification was carried out at 210° to 220° C. to obtain 4-behenoyloxyethyl-2,3,6,7-tetrahydro-1,4-diazocin-5-one.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346087 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-df1a55e079f2490d9fdb51575a250049 |
| 출처 메모 | uspto-grants-1982_08 |