Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl bromoacetate → 3-Methyl-4-oxo-2-phenyliminothiazolidine hydrobromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl bromoacetate | HCID 7748 | — |
| 반응물 | 1-Methyl-3-phenylthiourea | HCID 698294 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 3-Methyl-4-oxo-2-phenyliminothiazolidine hydrobromide | HCID 20527195 | — |
반응 단계
10 g of ethyl bromoacetate and 9.95 g of 1-methyl-3-phenylthiourea in 150 ml of acetone are boiled for 1 hour under a reflux condenser. The reaction mixture is allowed to cool and the crystals are filtered off and washed with acetone. Melting point 212°-215° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346088 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-807f3c22deb64f20afe079763f77af03 |
| 출처 메모 | uspto-grants-1982_08 |