Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sarcosine → 1-Methyl-3-n-nonyl hydantoin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sarcosine | HCID 1088 | — |
| 반응물 | Hydantoin | HCID 10006 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | capric N-chloramide | HCID 19040089 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | tert-Butanol | HCID 6386 | — |
| 생성물 | 1-Methyl-3-n-nonyl hydantoin | HCID 70549405 | 90% |
반응 단계
In accordance with the procedure described in Example 6, 41 g (0.2 mol) capric N-chloramide were reacted with sarcosine, sodium hydroxide in a mixture of tertiary butanol and water and then processed. The hydantoin remained in the aqueous solution was an oil, that was extracted with ether. The ether was removed by distillation to yield 43 g (90% yield) 1-methyl-3-n-nonyl hydantoin of the formula ##STR10## having the following analysis:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346233 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-37b99b25d34c4e0887d8172c6d4f7e0f |
| 출처 메모 | uspto-grants-1982_08 |