Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isopropanol → N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isopropanol | HCID 3776 | — |
| 반응물 | N-Methyl-D-glucamine | HCID 8567 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | lauric N-chloramide | HCID 19040106 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea | HCID 20527943 | 63% |
반응 단계
A mixture containing 7 g (30 mmol) of lauric N-chloramide dissolved in 200 ml of isopropanol, was reacted with a solution containing 5.85 g (30 mmol) of N-methyl-D-glucamine in 150 ml of isopropanol, 40 ml of water and 1.2 g (30 mmol) of sodium hydroxide at 50° C. for a period of 1 hour. The reaction mixture was processed in accordance with the procedures described in Example 12 to yield 7.38 g (63% yield) of N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea of the formula ##STR13## having a melting point of 109° C. and the following analysis:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346233 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-6e4c9133aa28410ebd9f602f512201ef |
| 출처 메모 | uspto-grants-1982_08 |