Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibenzylidene acetone → Tris(dibenzylideneacetone) palladium
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibenzylidene acetone | HCID 95417 | — |
| 반응물 | 1,5-Diphenylpenta-1,4-dien-3-one;palladium | HCID 154270 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Tris(dibenzylideneacetone) palladium | HCID 44556509 | — |
반응 단계
Bis-(dibenzylidene acetone) palladium (0.10 g; 0.17 mmole) was dissolved in methylene chloride (100 ml), and the solution filtered on a millepore filter to remove elemental palladium. Dibenzylidene acetone (0.51 mmole) was added to the solution, and the solution was stirred for 24 hours at ambient temperature. The solution was then evaporated to yield purple crystals of the tris-(dibenzylidene acetone) palladium product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04347232 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-bb8737df082d429b8775616499e8e7ff |
| 출처 메모 | uspto-grants-1982_08 |