Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Dichloroacetone → HCID 178479412, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Dichloroacetone | HCID 10793 | — |
| 반응물 | HCID 178513045 | HCID 178513045 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | HCID 178479412 | HCID 178479412 | — |
반응 단계
A suspension of amidinothiourea (16.8 g.) in acetone (75 ml.) was treated with 1,3-dichloroacetone (18 g.) in acetone (60 ml.). There was a slight exotherm and the crystalline suspension gradually changed to a fine white solid. After stirring overnight at room temperature the solid was filtered off and washed with acetone. Crystallization from ethanol gave 2-guanidino-4-chloromethylthiazole hydrochloride, m.p. 191°-193° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04347370 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-8f0590970f954d00939dac7949961f7e |
| 출처 메모 | uspto-grants-1982_08 |