Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroacetyl chloride → 2-Chloro-N-(4-chlorobenzenesulfonyl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroacetyl chloride | HCID 6577 | — |
| 반응물 | 4-Chlorobenzenesulfonamide | HCID 66824 | — |
| 생성물 | 2-Chloro-N-(4-chlorobenzenesulfonyl)acetamide | HCID 676503 | — |
반응 단계
The reactant N-chloroacetyl 4-chlorobenzene sulfonamide was prepared by mixing 30.0 g of 4-chlorobenzene sulfonamide and 60.0 ml of chloroacetylchloride. The mixture was refluxed for 6 hours, allowed to cool, and stand at room temperature overnight. The crystalline product was removed by filtration, washed repeatedly with hexane, and dried. The product consisted of 32.5 g of reactant (m.p. 122°-124° C.). Structure was confirmed by IR and NMR.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04347380 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-9157d1aad09d476e98fe686e61eee7f5 |
| 출처 메모 | uspto-grants-1982_08 |