Methanol → N-ethyl-3-methyl-6-nitroquinolin-2-amine

HRID 6805

반응식

HRID 6805 반응식
Cl[C:2]1[C:11]([CH3:12])=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([N+:13]([O-:15])=[O:14])[CH:8]=2)[N:3]=1.[CH2:16]([NH2:18])[CH3:17].CO>>[CH2:16]([NH:18][C:2]1[C:11]([CH3:12])=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([N+:13]([O-:15])=[O:14])[CH:8]=2)[N:3]=1)[CH3:17]

참가 물질

4

반응물 3

HCID 887MethanolHCID 6341EthylamineHCID 220190042-chloro-3-methyl-6-nitroQuinoline

생성물 1

HCID 22018880N-ethyl-3-methyl-6-nitroquinolin-2-amine

실험 절차

The product (1 g, 4.5 mmol) from Step A and a solution of 2N ethylamine in methanol (5 mL, 25 mmol) were used to prepare the product according to the procedure of Example 1, Step C.

후처리

  1. customto prepare the product

출처 및 근거

ORD 기록
ord-6fe6e3cc88c24bf59c2bd7d84afa2c25
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07084156B2

연결된 노트

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