Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylhydrazine → (E)-(2,4,6-trifluorophenyl)methylidenehydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylhydrazine | HCID 6061 | — |
| 반응물 | 2,4,6-Trifluorobenzaldehyde | HCID 521845 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | (E)-(2,4,6-trifluorophenyl)methylidenehydrazine | HCID 57917272 | — |
반응 단계
2,4,6-Trifluoro-benzaldehyde (x) (4.5 g, 27.3 mmol) was dissolved in Et2O, methylhydrazine was added (1.43 mL, 27.3 mmol) and the RM was stirred overnight. The solvent was evaporated and the solid residue was suspended in a mixture of pentane and EtOAc to afford after filtration the title compound as a bright yellow crystalline solid (tR 4.95 min (conditions 3), MH+=198.1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822468B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-cd338e979c4d47d48408e78b4dc0922f |
| 출처 메모 | uspto-grants-2014_09 |