Butanal → 3-[1-(1H-indol-3-yl)butyl]-1H-indole

HRID 6940

반응식

HRID 6940 반응식
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[CH:10](=O)[CH2:11][CH2:12][CH3:13]>CO.O>[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([CH:10]([C:3]2[C:4]3[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=3)[NH:1][CH:2]=2)[CH2:11][CH2:12][CH3:13])=[CH:2]1

참가 물질

5

반응물 2

HCID 261ButanalHCID 798Indole

생성물 1

HCID 102661333-[1-(1H-indol-3-yl)butyl]-1H-indole

시약·촉매·용매 2

HCID 887Methanol용매HCID 962Water용매

실험 절차

282 mg of indole (2.4 mmol) were dissolved in 10 ml of CH3OH and 5 ml of H2O; 72 mg (1 mmol) of butyraldehyde and 240 mg of dysprosium triflate-(CF3SO3)3Dy-(0.393 mmol) were added.

출처 및 근거

ORD 기록
ord-a7069c89951542c6aac014e0ba0b4104
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07084166B2

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