4-Bromoaniline → 2-(4-bromophenyl)-6-butoxy-3,4-dihydro-2H-isoquinolin-1-one

HRID 69456

반응식

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH2:8])=[CH:4][CH:3]=1.[CH2:9]([O:13][C:14]1[CH:22]=[CH:21][C:17]([C:18](Cl)=[O:19])=[C:16]([CH2:23][CH2:24]Cl)[CH:15]=1)[CH2:10][CH2:11][CH3:12]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:24][CH2:23][C:16]3[C:17](=[CH:21][CH:22]=[C:14]([O:13][CH2:9][CH2:10][CH2:11][CH3:12])[CH:15]=3)[C:18]2=[O:19])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 78074-Bromoaniline

HCID 534401334-Butoxy-2-(2-chloroethyl)benzoyl chloride

생성물 1

HCID 689911152-(4-bromophenyl)-6-butoxy-3,4-dihydro-2H-isoquinolin-1-one

실험 절차

According to Method A, 4-bromo-phenylamine was reacted with 4-butoxy-2-(2-chloroethyl)-benzoyl chloride. In this way the product was obtained with molecular weight 374.28 (C19H20BrNO2); MS (ESI): 374 (M+H+).

후처리

customIn this way the product was obtained with molecular weight 374.28 (C19H20BrNO2)

출처 및 근거

ORD 기록: ord-0ce0a7a5fbc149c4a58b526ad48469b4
출처 데이터셋: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08822495B2

연결된 노트

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