Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-4-chloro-6-methylpyrimidine → HCID 58395746, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-4-chloro-6-methylpyrimidine | HCID 21810 | — |
| 반응물 | Di-tert-butyl dicarbonate | HCID 90495 | — |
| 촉매 | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| 생성물 | HCID 58395746 | HCID 58395746 | — |
반응 단계
Method 24 was followed using 4-chloro-6-methylpyrimidin-2-amine (1.0 equiv.), BOC2O (2.0 equiv.), and DMAP (cat.) to afford 4-chloro-N,N-di-BOC-6-methylpyrimidin-2-amine in 71%. LCMS (m/z): 344.2 (MH+); LC Rt=4.3 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822497B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-4e69f75b88c7414ba88fdc4f50c19346 |
| 출처 메모 | uspto-grants-2014_09 |