Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Aminobenzothiazole → 4-Nitrophenyl benzo[d]thiazol-6-ylcarbamate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Aminobenzothiazole | HCID 68288 | — |
| 반응물 | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-Nitrophenyl benzo[d]thiazol-6-ylcarbamate hydrochloride | HCID 66797303 | 81% |
반응 단계
6-Aminobenzothiazole (100 mg, 0.666 mmol) and p-nitrophenyl chloroformate (148 mg, 0.733 mmol) were stirred at rt in CH2Cl2 (5 mL) overnight. The resulting solid was collected by filtration, yielding 183 mg (81%) of the title compound. LC-MS: RT=8.17 min, [M+H]+=316.0.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822472B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-5b5b00a8a2234c6e86c3e37c49c0c5b4 |
| 출처 메모 | uspto-grants-2014_09 |