Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
cis-2-Aminocycloheptanecarboxylic acid methyl ester → HCID 69655884, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | cis-2-Aminocycloheptanecarboxylic acid methyl ester | HCID 1512672 | — |
| 반응물 | Water ammonium hydroxide | HCID 86589665 | — |
| 생성물 | HCID 69655884 | HCID 69655884 | — |
반응 단계
cis-2-Aminocycloheptanecarboxylic acid methyl ester (1.65 g, 9.64 mmol) was treated with 20 mL of NH4OH/H2O and stirred at room temperature for 24 h. The solution was concentrated in vacuo and azeotroped once with toluene. The reaction afforded 2.20 g of cis-2-aminocycloheptanecarboxylic acid amide as a white solid: 1H NMR (DMSO-d6) δ 7.81 (m, 3 H), 7.20 (s, 1 H), 2.76 (m, 1 H), 1.68–1.40 (m, 11 H); MS m/e 157.28 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07084178B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-02ef1dfe6f1a403686e87c22720d628b |
| 출처 메모 | uspto-grants-2006_08 |